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Modern Nuclear Chemistry, by W.D. Loveland, D.J. Morrissey, and G.T. Seaborg Copyright # 2006 John Wiley & Sons, Inc.

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Hyper Raman scattering signals are typically five to seven orders of magnitude weaker than those of linear Raman scattering. Larger hyper Raman signals are observed under resonant conditions (Washington et al., 1977; Ziegler and Roebber. 1987) and in surfaceenhanced hyper Raman scattering (Murphy et al., 1982; Golab et al., 1988; Nie et al., 1990). Since hyper Raman scattering is an incoherent process which does not require phase matching, it is preferentially observed at an angle of 90 from the incident laser direction. As for any spontaneous phenomenon, a double monochromator is used in most cases. Initial hyper Raman spectra were generated with a Q-switched ruby laser nperating at approx. 1 Hz (Terhune et al., 1965) and detected with a synchronously gated photomultiplier tube and subsequently with optical multichannel detection (Verdieck et al., 1970; Savage and Maker, 1971; French and Long, 1975). The use of cw pumped acousto-optically Q-switched Nd:YAG lasers (repetition rates of 5 kHz), synchronously gated photomultiplier tubes (Vogt, 1976; Schmid and Schrotter, 1977), and synchronously gated two-dimensional single-photon counting detectors (Vogt, 1987; Acker et al., 1989) has improved the signal-to-noise ratio of hyper Raman spectra. Considerable further improvements have been obtained with mode-locked pulses (at 82 MHz) from a Nd:YAG laser to observe the surface-enhanced hyper Raman signal from pyridine adsorbed on silver (Golab et a]., 1988). In these studies hyper Raman signals were observed with intensities close to spontaneous Raman scattering. They showed that surface enhanced hyper Raman scattering (SEHRS) has become a useful spectroscopic technique. In view of the recent advances in laser and detector technology, significant improvement in SEHRS sensitivity will come rapidly from the use of an intensified CCD camera for hyper Raman signal detection and the use of a continuously tunable mode-locked Ti:Sapphire laser as the excitation source (Yu and Nie, 1992).

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